2022年 06期

X射线荧光光谱法检测用聚合物基标准物质的制备

Preparation of Polymer-based Standard Substance Used in Verification by X-ray Fluorescence Spectrometry


摘要(Abstract):

以热塑性树脂为熔剂,金属氧化物为金属元素载体,采用双螺杆熔融共混结合注塑挤出成型工艺,制备X射线荧光光谱法检测用聚合物基标准物质;采用扫描电子显微镜、能量色散X射线谱、同步热重分析等手段对标准物质进行表征。结果表明,聚乙烯基标准物质金属元素分布最均匀,高温烧蚀测试样品中金属氧化物含量与理论添加量误差小于0.6%,最大拉伸强度达12 MPa,初始热分解温度高于290℃,样品表面最大水接触角为91°,具有优异的力学性能、耐热性和疏水性。

关键词(KeyWords): 热塑性聚合物;复合材料;标准物质;X射线荧光光谱法

基金项目(Foundation): 国家自然科学基金项目(21704033);; 中国博士后科学基金项目(2019M662441)

作者(Author):鲁毅,陈建,郭国建,柳洪超,董俊伟,由欣然,宗传永

DOI: 10.13349/j.cnki.jdxbn.20220914.001

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